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Raising the Bar for Analytical Excellence™

Publications

The following is a list of publications associated with TBAR or its personnel:

Brown, P.N., Paley, L.A., Roman, M.C., Chan, M. Single Laboratory Validation of a Method for the Detection and/or Quantification of Select Alkaloids in Goldenseal Supplements and Raw Materials by Reversed-Phase High Performance Liquid Chromatography, Pharmaceutical Biology, in press.

Orozco, D., Skamarack, J., Reins, K., Titlow, B., Lunetta, S., Li, F., Roman, M. Determination of Ubidecarenone (Coenzyme Q-10, Ubiquinol-10) in Raw Materials and Dietary Supplements by HPLC-UV: Single Laboratory Validation, J. AOAC Int., in press.

Thomas, J.B., Sharpless, K.E., Mitvalsky, S., Roman, M., Yen, J., Satterfield, M.B. Determination of Caffeine and Caffeine-Related Metabolites in Ephedra-Containing Standard Reference Materials Using Liquid Chromatography with Absorbance Detection and Tandem Mass Spectrometry, J. AOAC Int., 90 (2007) 934-940.

Ji, D., Roman, M.C., Zhou, J., Hildreth, J. Determination of Chondroitin Sulfate in Raw Materials and Dietary Supplements by HPLC-UV after Enzymatic Hydrolysis: Single Laboratory Validation, J. AOAC Int., 90 (2007) 659-669.

Roman, M.C, Betz, J.M., Hildreth, J. Determination of Synephrine in Bitter Orange Raw Materials, Extracts, and Dietary Supplements by HPLC-UV: Single Laboratory Validation, J. AOAC Int., 90 (2007) 68-81.

Sharpless, K. E., Anderson, D. L., Betz, J. M., Butler, T. A., Capar, S. G., Cheng, J., Fraser, C., Gay, M., Gardner, G., Howell, D., Ihara, T., Lam, J., Long, S., McCooeye, M., Mackey, E. A., Mindak, W., Mitvalsky, S., Murphy, K., Phinney, K. W., NguyenPho, A., Porter, B. J., Roman, M., Sander, L. C., Satterfield, M., Scriver, C., Sturgeon, R. E., Brown Thomas, J., Vocke, R., Wise, S. A., Wood, L. J., Yang, L., Yen, J. H., and Ziobro, G. Preparation and Characterization of a Suite of Ephedra-Containing Standard Reference Materials, J. AOAC Int., 89 (2006) 1483-1495.

Jaksch, F., Roman, M., Wang, M. “Handbook of Analytical Methods for Dietary Supplements,” American Pharmacists Association, 2006.

Roman, M. The AOAC Validation Effort for Dietary Supplements, Nutraceutical World, 8 (2005) 82 – 86.

Sander, L.C., Sharpless, K.E., Satterfield, M.B., Ihara, T., Phinney, K.W., Porter, B.J., Yen, J., Wise, S.A., Gay, M.L., Sturgeon, R., Lam, J.W., McCooeye, M., Gardner, G., Fraser, C., and Roman, M. Determination of Ephedrine Alkaloids in Dietary Supplement Standard Reference Materials, Analytical Chemistry, 77 (2005) 3101 - 3112.

Roman, M.C. Determination of ephedrine alkaloids in botanicals and dietary supplements by HPLC-UV: collaborative study. J. AOAC Int. 87 (2004) 1 – 14.

Roman, M.C. Determination of ephedra alkaloids in urine and plasma by HPLC-UV: collaborative study. J. AOAC Int. 87 (2004) 15-24.

Roman, M.C. and Brown, P.R. Free Flow Electrophoresis as a Preparative Separation Technique: Theory, Instrumentation and Applications. Analytical Chemistry, 66 (1994) 86A-94A.

Painuly, P. and Roman, M.C. A New Method for Scaling up Free Flow Electrophoresis. Applied and Theoretical Electrophoresis, 3 (1993) 119-127.

Tarnopolsky, Y., Roman, M.C. and Brown, P.R. A New Approach to Scaling up Electrophoresis. Separation Science and Technology, 28 (1993) 719-731.

Roman, M. and Brown, P.R. Separation Techniques for Biotechnology in the 1990s. Journal of Chromatography, 592 (1992) 3-12.

Roman, M.C. and Siergiej, R.W. Accuracy of Computer-Simulated Gas Chromatographic Separations Based on a Linear Elution Strength Model. Journal of Chromatography, 589 (1992) 215-222.

Abbay, G.N., Barry, E.F., Leepipatpiboon, S., Ramstad, T., Roman, M.C., Siergiej, R.W., Snyder, L.R. and Winniford, W.L. Practical Applications of Computer Simulation for Gas Chromatography Method Development. LC-GC, 9 (1991) 100-114.